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Explore the rheological properites of minerals at extreme conditions

Rheology Grand Challenge I

Rheology Grand Challege group was formed in 2002 and funded by National Science Foundation for five years. RGC is renewed in year 2007 for another five year duration.

 

The DDIA was designed just prior to the beginning of the RGC phase I program (DURHAM et al., 2002b; WANG et al., 2003a). The prototype system was built by Livermore Labs under the supervision of Durham. The first experiments at a synchrotron were carried out at Brookhaven National Labs during RGC phase I in 2002. Based on the success of this system, three more DDIAs have been built, one which remains at Brookhaven Labs, one at GSECARS in Chicago, and one with Green at UC Riverside. Another has been built at the Bayerisches Geoinstitut in Bayreuth, Germany. The original Livermore DDIA is now at Minnesota with Mei and Kohlstedt. The DDIA is derived from the Japanese designed DIA, a cubic anvil system that compresses a cubic assembly with a single hydraulic ram. Such a device has been running routinely at the NSLS beamline since about 1990 and at GSECARS since their beginning. The DDIA modification adds two rams, one to drive the top anvil and one for the bottom. With three rams in place one can maintain a constant pressure with the main ram as the differential rams push to shorten the entire sample assembly. The solid medium sample assembly includes pistons, usually made of corundum, that transmit the force of the deforming anvils to the sample as a differential stress. Since stress and strain are measured directly in the sample, the strength of the pressure medium is not important, only the sample stress vs strain rate. The sign of the deforming stress in this system can be reversed by retracting the deforming rams. This feature adds to the flexibility of the DDIA.

The rotational Drickamer (RDA) is a modified version of Drickamer apparatus in which a rotational actuator is added to a conventional Drickamer apparatus (Fig. 4). After pressurization (and heating), one of the anvils can be rotated causing shear strain to a sample. The motivation for the design of this apparatus was twofold: (i) because of its design, the support for anvils in a rotational Drickamer apparatus is nearly identical to that of a conventional Drickamer apparatus for static experiments. Consequently, one can conduct deformation experiments under the P-T conditions similar to those for static experiments. Using a tungsten carbide anvils, deformation experiments have been performed to ~18 GPa, ~1800 K (stability field of ringwoodite), (ii) also because of the geometry of deformation, there is no limitation in the maximum strain.

(left) Schematic of the DDIA by Bill Durham. The DDIA high pressure device is driven by one main ram indicated by the big arrows. This ram drives the top and bottom anvils together and the side anvils (2 of the 4 are illustrated) are driven into the sample chamber by a wedge type effect. The upper and lower anvils have each an additional ram that can drive them independently of the main ram and hence independently of the side anvils. During deformation, the main ram may need to be backed off of the sample in order to maintain a constant pressure (which can be monitored by the diffraction observations).

(middle) A RDA installed at Yale mineral physics lab.

(right) Cell design for the double-stage (6/2) configuration tested in the DDIA by GSECARS. In DDIA-30, the cubic cell will be about 35 mm edge length and the second-stage Drickamer anvils will be 10 mm in diameter.